Synthesis, Structure, Hirshfeld surface analysis and Anti-oxidant studies on 2-(4-dimethylamino) benzylidene) hydrazine-1-carbothioamide
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| 1. | Title | Title of document | Synthesis, Structure, Hirshfeld surface analysis and Anti-oxidant studies on 2-(4-dimethylamino) benzylidene) hydrazine-1-carbothioamide |
| 2. | Creator | Author's name, affiliation, country | P. T. Ndifon; University of Yaoundé 1; Cameroon |
| 2. | Creator | Author's name, affiliation, country | L. E. Tsakeng Ngoudjou; University of Yaoundé 1; Cameroon |
| 2. | Creator | Author's name, affiliation, country | A. Pamen Yepseu; University of Yaounde 1; Cameroon |
| 2. | Creator | Author's name, affiliation, country | A. Gbambie Paboudam; University of Yaounde 1; Cameroon |
| 2. | Creator | Author's name, affiliation, country | A. L. Mbani; University of Yaounde 1; Cameroon |
| 2. | Creator | Author's name, affiliation, country | P. Boulet; Institut Jean LAMOUR; France |
| 2. | Creator | Author's name, affiliation, country | F. Cleymand; Institut Jean LAMOUR; France |
| 3. | Subject | Discipline(s) | |
| 3. | Subject | Keyword(s) | Thiosemicarbazone, p-dimethylaminobenzaldéhyde, Crystal structure, antioxidant activity, Spectroscopic methods. |
| 4. | Description | Abstract | The crystallographic structure of the Schiff base, 2-(4-dimethylamino) benzylidene)hydrazine-1-carbothioamide (H1L) is reported from X-ray single crystal data. The crystal structure is a triclinic crystal unit cell, space group P-1(2) with a = 8.529(3) Å, b = 9.387(4) Å, c =15.538(6) Å, alpha = 73.926(12) °, beta = 79.730(12) °, gamma = 83.087(13) °, V = 1174.2(8) Å 3 and Z = 4. The Hirsfield surface analysis revealed the presence of π…π stacking and N-H…π interactions. The title compound (H1L) was synthesized by the condensation reaction of thiosemicarbazide, and p-dimethylaminobenzaldéhyde and characterized using microanalysis, FT-IR, UV-Visible, 1H-NMR, 13C-NMR, HMBC, COZY, NOESY and used to investigate their antioxidant potency. Antioxidant activity of H1L shows that the potency of the Schiff base is comparable to that of vitamin C. |
| 5. | Publisher | Organizing agency, location | |
| 6. | Contributor | Sponsor(s) | This work received financial assistance under the “Fond Spéciale pour la Modernization de la Recherche Universitaire au Cameroun” (Decree n° 2009/121 of 8 April 2009). |
| 7. | Date | (YYYY-MM-DD) | 01-08-2023 |
| 8. | Type | Status & genre | Peer-reviewed Article |
| 8. | Type | Type | |
| 9. | Format | File format | |
| 10. | Identifier | Uniform Resource Identifier | https://revues.imist.ma/index.php/morjchem/article/view/38955 |
| 10. | Identifier | Digital Object Identifier (DOI) | https://doi.org/10.48317/IMIST.PRSM/morjchem-v11i04.38955 |
| 11. | Source | Title; vol., no. (year) | Moroccan Journal of Chemistry; Vol 11, No 04 (2023): pp. 897-1318 |
| 12. | Language | English=en | en |
| 13. | Relation | Supp. Files | |
| 14. | Coverage | Geo-spatial location, chronological period, research sample (gender, age, etc.) | |
| 15. | Rights | Copyright and permissions |
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