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RHEOLOGIC STUDY AND THERMAL BEHAVIOR OF A NEW SULPHURATED AND PHOSPHOROUS TRI-FUNCTIONAL EPOXY RESIN.


 
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1. Title Title of document RHEOLOGIC STUDY AND THERMAL BEHAVIOR OF A NEW SULPHURATED AND PHOSPHOROUS TRI-FUNCTIONAL EPOXY RESIN.
 
2. Creator Author's name, affiliation, country N. Elaouni; Laboratoryof Polymer, Radiation and Environment (LPRE), Team of Chemistry Organic and Macromolecular (TCOM), Department of Chemistry, Faculty of Sciences, University Ibn Tofail.B.P.133, 14000, Kenitra, Morocco.; Morocco
 
2. Creator Author's name, affiliation, country J. El azzaoui
 
2. Creator Author's name, affiliation, country A. El Harfi
 
3. Subject Discipline(s)
 
3. Subject Keyword(s) rheologic Study, Tri-functional Sulphurated and Phosphorous epoxide resin, Microscopic characterization, Thermo-gravimetric Study.
 
4. Description Abstract

In this work, we presented the synthesis of a new sulphurated and phosphorous tri-functional epoxide resin. To reach this result, we proceeded to the synthesis, in a first stage, of a precursor of the epoxide matrix. In the second stage, it would consist in the fictionalization of the precursor by means of the épichloridrine. The microscopic characterization of the synthesized resin was confirmed by the Fourier Transform Infrared (FTIR) and by nuclear magnetic Résonnance (NMR) 1H, 13C, 31P. The epoxy tri-functional polymer was then reticulated thermically by the methyl alcohol dianiline( MDA). Its reactivity towards resin was characterized by a rheologic study. The study of composite material by means of the thermo-gravimetric analysis allowed us to estimate and to estimate the character of the thermal degradation of this new macromolecular chain.

Keywords: rheologic Study, tri-functional sulphurated and phosphorous epoxide resin, microscopic characterization, thermo-gravimetric Study.

 
5. Publisher Organizing agency, location
 
6. Contributor Sponsor(s)
 
7. Date (YYYY-MM-DD) 14-01-2016
 
8. Type Status & genre Peer-reviewed Article
 
8. Type Type
 
9. Format File format PDF
 
10. Identifier Uniform Resource Identifier https://revues.imist.ma/index.php/morjchem/article/view/3481
 
10. Identifier Digital Object Identifier (DOI) https://doi.org/10.48317/IMIST.PRSM/morjchem-v4i1.3481
 
11. Source Title; vol., no. (year) Moroccan Journal of Chemistry; Vol 4, No 1 (2016)
 
12. Language English=en en
 
13. Relation Supp. Files
 
14. Coverage Geo-spatial location, chronological period, research sample (gender, age, etc.)
 
15. Rights Copyright and permissions Copyright (c)