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Characterization of Eggshell Combination with Activated Corn Cob as Ion Pb2+ Adsorbent through a Batch Process


 
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1. Title Title of document Characterization of Eggshell Combination with Activated Corn Cob as Ion Pb2+ Adsorbent through a Batch Process
 
2. Creator Author's name, affiliation, country Sri Mulyani, Nanda Putri Pertiwi, Budi Utami; Morocco
 
3. Subject Discipline(s)
 
3. Subject Keyword(s) Adsorption, Corn cob, Egg shell, Pb metal
 
4. Description Abstract This study aims to determine the characteristics of the combination of corn cobs and eggshells as Pb metal adsorbents. In this research, adsorption using the Batch method. This research uses an experimental approach in the laboratory. This experiment has four stages: adsorbent preparation, adsorbent activation, characterization of adsorbent functional groups using FTIR, and characterization of adsorbent to adsorb the ion Pb2+. The adsorption isotherm was determined using the Langmuir, Freundlich, Temkin and Dubinin-Radushkevich isotherm patterns. While the determination of adsorption effectivity through optimum conditions on variations in adsorbent composition, adsorbent mass, contact time, and the effect of initial concentration of Pb metal on adsorption capacity are carried out using AAS. The results showed that the adsorbent combination of corn cobs and eggshells contained OH, CaCO32- groups, cellulose and protein constituent groups that played a role in the adsorption process, using the Langmuir isotherm pattern, which means the adsorption process takes place chemically. The optimum composition ratio of the adsorbent corn cobs and eggshells is 1: 2, the optimum mass of adsorbent was 0.2 g, and the contact time optimum is 60 minutes, with the optimum percentage of Pb2+ adsorbed in those conditions are 94.49%, 98.69 %, 99.03%, respectively. The more the initial concentration of Pb metal, the greater the adsorption capacity, and in this study, the largest adsorption capacity at a concentration of 30 ppm with a value of 1.393445 mg/g.
 
5. Publisher Organizing agency, location
 
6. Contributor Sponsor(s)
 
7. Date (YYYY-MM-DD) 26-05-2022
 
8. Type Status & genre Peer-reviewed Article
 
8. Type Type
 
9. Format File format PDF
 
10. Identifier Uniform Resource Identifier https://revues.imist.ma/index.php/morjchem/article/view/32647
 
10. Identifier Digital Object Identifier (DOI) https://doi.org/10.48317/IMIST.PRSM/morjchem-v10i2.32647
 
11. Source Title; vol., no. (year) Moroccan Journal of Chemistry; Vol 10, No 2 (2022)
 
12. Language English=en en
 
13. Relation Supp. Files
 
14. Coverage Geo-spatial location, chronological period, research sample (gender, age, etc.)
 
15. Rights Copyright and permissions Copyright (c) 2022 Moroccan Journal of Chemistry