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Synthesis of V-shaped Schiff base ligand of type (N1E,N2E)-N1,N2-bis(pyridin-2-yl-methylene)-ethane-1,2-diamine, DFT/XRD/HAS analysis


 
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1. Title Title of document Synthesis of V-shaped Schiff base ligand of type (N1E,N2E)-N1,N2-bis(pyridin-2-yl-methylene)-ethane-1,2-diamine, DFT/XRD/HAS analysis
 
2. Creator Author's name, affiliation, country Ismail kh Warad; nnu
 
3. Subject Discipline(s)
 
3. Subject Keyword(s) Crystal structures; DFT calculations; Hirshfeld surface.
 
4. Description Abstract

A new functionalized V-shaped Schiff base (N1E,N2E)-N1,N2-bis(pyridin-2-ylmethylene)ethane-1,2-diamine ligand was synthesized in good yield via condensation of picolinaldehyde with ethane-1,2-diamine in ethanol solution under open reflux condition. The prepared N4-SB was characterized by XRD single crystal then computed via Hirshfeld surface analysis (HSA). Moreover, the two-dimensional fingerprint (2D-FP) and structural DFT optimization processes were also performed. The DFT structural parameters like bonds and angles lengths were matching with their XRD experimental relatives.

 
5. Publisher Organizing agency, location
 
6. Contributor Sponsor(s)
 
7. Date (YYYY-MM-DD) 27-04-2020
 
8. Type Status & genre Peer-reviewed Article
 
8. Type Type
 
9. Format File format PDF
 
10. Identifier Uniform Resource Identifier https://revues.imist.ma/index.php/morjchem/article/view/20565
 
10. Identifier Digital Object Identifier (DOI) https://doi.org/10.48317/IMIST.PRSM/morjchem-v8i3.20565
 
11. Source Title; vol., no. (year) Moroccan Journal of Chemistry; Vol 8, No 3 (2020)
 
12. Language English=en en
 
13. Relation Supp. Files
 
14. Coverage Geo-spatial location, chronological period, research sample (gender, age, etc.)
 
15. Rights Copyright and permissions Copyright (c) 2020 Moroccan Journal of Chemistry