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Preparation and characterization of ceramic sol–gel composite coatings - densification temperature optimisation -


 
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1. Title Title of document Preparation and characterization of ceramic sol–gel composite coatings - densification temperature optimisation -
 
2. Creator Author's name, affiliation, country Ouafa TAHIRI ALAOUI; Département de chimie, Faculté des Sciences et Techniques, Université My Ismail, BP 509 Boutalamine, Errachidia, Morocco
 
2. Creator Author's name, affiliation, country Matthieu TOUZIN; Unité Matériaux et Transformations, Université de Lille 1- Bâtiment C6, 59655 Villeneuve d’Ascq
 
2. Creator Author's name, affiliation, country Franck BECLIN; Unité Matériaux et Transformations, Université de Lille 1- Bâtiment C6, 59655 Villeneuve d’Ascq
 
3. Subject Discipline(s)
 
3. Subject Keyword(s) sol-gel processing, coating, thermal treatment, hardness, sodium chloride.
 
4. Description Abstract Thick (~ 25 µm) ceramic coatings on porous ceramic substrates were elaborated by means of dispersing alumina and rutile powders in a silica sol-gel solution. Resulting coatings, which present a composite structure consisting in Al2O3 and TiO2 grains embedded in an amorphous SiO2 matrix, demonstrate a good adhesion to the substrate and a real improvement of its surface by closing the porosity and also reducing the roughness. Mechanical characterization by micro-indentation showed an increase of the coating hardness when the thermal treatment temperature increases. This hardness increase is attributed to the densification of the coating that proceeds by grain rearrangement thanks to the sol-gel derived silica phase viscosity decrease during the thermal treatment. In order to decrease the coating densification temperature, the silica intergranular phase was modified by incorporating Na+ ions in its structure. This was done by adding NaCl salt in the sol-gel solution and leads to the decrease of the densification temperature.
 
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7. Date (YYYY-MM-DD) 01-08-2014
 
8. Type Status & genre Peer-reviewed Article
 
8. Type Type
 
9. Format File format PDF
 
10. Identifier Uniform Resource Identifier https://revues.imist.ma/index.php/MJCM/article/view/2112
 
11. Source Title; vol., no. (year) Moroccan Journal of Condensed Matter; Vol 16, No 1 (2014)
 
12. Language English=en en
 
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15. Rights Copyright and permissions Copyright (c)