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We present the experimental results of (Co_xZn_1-x/Cu)n multilayers (3<x<10) grown using the electrochemical dual bath method. The X-ray diffraction patterns have shown that the CoZn structural lattice parameters are close to those of the monoclinic CoZn₁₃ compound.

We have developed an analytical model in the X-ray kinematical theory adapted to the electrodeposited (Co_xZn_1-x/Cu) multilayers. We have shown that the model can give interesting structural information about the multilayer components, and reproduces the position of the satellite peaks around the main diffraction peak. Thus we have deduced the multilayer period and performed comparison between experimental results and the analytical model. The magnetic properties at room temperature reveal both superparamagnetic and ferromagnetic features. The inclusion of Zn into the magnetic layer and the existence of CoZnCu based alloy at the interfacial regions explain the magnetic properties. The magnetoresistance (MR) loop displays a broad , rounded maximum and the saturation is not observed even at high applied fields. The MR(H) behaviour and its small ratio can be attributed to interfacial effects.