Gas Chromatography-Mass Spectrometry Analysis and Comparison of Volatile Components Obtained by Hydrodistillation and Headspace Solid Phase Microextraction (HS-SPME) from Teucrium luteum subsp. flavovirens

Mohamed ZNINI, Omar Ou-Ani, Driss Chebabe, jean Costa, Lhou Majidi

Abstract


The main purpose of this work is to investigate the comparative chemical analysis of essential oil (EO) isolated by hydrodistillation (HD) and volatile fraction (VF) detected by headspace solid-phase micro-extraction (HS–SPME) obtained from Teucrium luteum subsp. flavovirens using Gas Chromatography–Retention Indices (GC-RI) and GC–Mass Spectrometry (GC-MS). 63 volatile compounds identified in hydrodistilled essential oil (HD), representing 89.9% of the total oil, while HS-SPME revealed 50 components constituting 99.3% of the volatile material. The chemical composition of EO comprised mainly of of oxygenated sesquiterpenes (48.6%) while, hydrocarbon monoterpenes were detected in higher concentrations in VF (54.1%). The comparative analysis of two chemoprofiles obtained by two methods shows quantitative and semi-qualitative differences. The current study is the first report involving rapid analysis of volatile components of T. luteum subsp. flavovirens by HS-SPME.


Keywords


Teucrium luteum subsp. flavovirens, Essential oil, Volatile fraction, Hydrodistillation, Headspace solid-phase micro-extraction

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DOI: https://doi.org/10.48347/IMIST.PRSM/ajmap-v8i1.28536

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ISSN: 2458-5920